Research on preparation and performance of ceramic denture materials applied for three dimensional printing_Journal of Biomedical Engineering

Authors：

ZHOU Jing ^1,2,3 ,  DUAN Guolin ¹

1. School of Mechanical Engineering, Hebei University of Technology, Tianiin 300130, P.R.China;
2. School of Mechanical Engineering, Tianjin University of Science & Technology, Tianjin 300222, P.R.China;
3. Tianjin Key Laboratory of Integrated Design and On-line Monitoring for Light Industry & Food Machinery and Equipment, Tianjin 300222, P.R.China;

Corresponding author：

DUAN Guolin, Email: glduan@hebut.edu.cn

Keywords：

micro-flow extrusion; ceramic slurry; rheological property; sintering; mechanical property

DOI：

10.7507/1001-5515.201607023

Video：

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The micro-flow extrusion forming of ceramic material has not been developed in three dimensional (3D) printing field. The shape forming of material is by bonding and stacking of filaments of ceramic slurry extruded through micro-sized pores with rather large gaps and porosities, which can affect material’s density after sintering and its mechanical property thereafter. Aiming at such a deficiency of this process, the preparation method of ceramic denture printing paste applicable to the process is studied, and the properties of slurry and sintering performance are analyzed and tested. It is concluded that the rheological properties of the prepared ceramic slurry conforms the requirement of micro-flow extrusion process, and the green body after sintering can satisfy the mechanical property requirement of oral denture. This is a technologic breakthrough, laying a foundation for the application of micro-flow extrusion forming in 3D printing of ceramic material, and promoting its development and maturation.

Citation： ZHOU Jing, DUAN Guolin. Research on preparation and performance of ceramic denture materials applied for three dimensional printing. Journal of Biomedical Engineering, 2017, 34(6): 914-921. doi: 10.7507/1001-5515.201607023 Copy

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10.	葛泳, 纪箴, 黄敏, 等. 掺杂氧化物对 ZrO₂ 相结构稳定性及烧结性能的影响. 北京科技大学学报, 2012, 34(3): 305-309.
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12.	刘振英, 赵金虎, 宋雪洋, 等. 烧结方式对氧化铝-氧化锆复相陶瓷性能的影响. 人工晶体学报, 2015, 44(5): 1289-1293.
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1. Wang J W, Shaw L L. Rheological and extrusion behavior of dental porcelain slurries for rapid prototyping applications. Materials Science and Engineering: A, 2005, 397(1/2): 314-321.
2. 李小倩. 基于 MAM 自由成形技术的 ZrO₂ 全瓷牙冠制备工艺研究. 武汉: 华中科技大学, 2013.
3. 伍权, 张祥林, 吴斌, 等. 基于挤出沉积成形技术的多孔生物支架制备. 华中科技大学学报:自然科学版, 2011, 39(12): 33-36.
4. Zhu Dongbin, Xu Anping, Qu Yunxia, et al. Functionalized bio-artifact fabricated via selective slurry extrusion. Part 1: preparation of slurry containing tourmaline superfine powders. J Nanosci Nanotechnol, 2011, 11(12): 10891-10895.
5. 刘洪军, 李烨, 翟亚楠. 水基牙科 3Y-ZrO₂ 浆料的制备工艺研究. 中国陶瓷, 2014, 50(6): 63-67.
6. 王翠凤, 简佑泽. 氧化锆微小孔注射成形研究. 长春工程学院学报:自然科学版, 2013, 14(4): 125-128.
7. 卢振, 张凯锋, 王振龙. 粉末微注射成形 ZrO₂ 微结构表面质量控制. 材料科学与工艺, 2010, 18(1): 129-132.
8. 许勇, 孙国庆, 汪仁. ZrO₂ 的烧结动力学研究. 天然气化工, 1994, 19: 14-17.
9. 罗志安, 肖建中. 氧化锆流延基片的烧结温度及其性能研究. 武汉科技大学学报: 自然科学版, 2009, 32(2): 173-177.
10. 葛泳, 纪箴, 黄敏, 等. 掺杂氧化物对 ZrO₂ 相结构稳定性及烧结性能的影响. 北京科技大学学报, 2012, 34(3): 305-309.
11. 陈静, 黄晓巍, 覃国恒. 两步烧结法制备纳米氧化钇稳定的四方氧化锆陶瓷. 硅酸盐学报, 2012, 40(3): 335-339.
12. 刘振英, 赵金虎, 宋雪洋, 等. 烧结方式对氧化铝-氧化锆复相陶瓷性能的影响. 人工晶体学报, 2015, 44(5): 1289-1293.
13. 王翠凤, 邱锡荣, 王珉玟, 等. 氧化锆微注射成形工艺参数. 粉末冶金材料科学与工程, 2012, 17(6): 712-718.
14. 国家食品药品监督管理局. YY 0716-2009 牙科陶瓷. 北京: 国家食品药品监督管理局, 2009.
15. ISO. ISO 6872-2015: Dentistry-Ceramic materials. Switerland: ISO, 2015.

Journal of Biomedical Engineering

Research on preparation and performance of ceramic denture materials applied for three dimensional printing

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